HALAL ACCREDITATION
CERTIFICATE

Fruits and vegetables with High Water and High Acid Content

Detection and Quantification Analysis of Selected Pesticides

GC-MS/MS Method

[Number of Selected Pesticides Analyzed is 174  

2-Phenylphenol (Ortho phenylphenol); 2,4-DDD; 2,4-DDE; DDT (the sum of p,p'-DDT, o,p'-DDT, p-p'-DDE and p,p'-TDE (DDD) in DDT); Acephate; Acetochlor; Acibenzolar-S-methyl; Aclonifen; Alachlor; Aldrin and Dieldrin (combination of Aldrin and Dieldrin, calc. as Dieldrin); Bifenthrin (sum of isomers); HCH- alpha (Hexachlorocyclohexane-alpha); Anilofos; Azinphos-ethyl; Azinphos-methyl; Benfluralin; HCH-beta (Hexachlorocyclohexane-beta); Bifenazate; Bifenthrin; Bioresmethrin; Biphenyl; Bromophos-ethyl; Bromophos (Bromophos-methyl); Bromopropylate; Bromuconazole; Cadusafos; Captan (the sum of Captan and THPI, calc. as Captan); Chlorbufam; Chlordane (the sum of cis- ve trans-chlordane isomers); Chlorfenapyr; Chlorfenson; Chlorfenvinphos; Chloroneb; Chlorothalonil; Chlorpropham; Chlorpyrifos; Chlorpyrifos-methyl; Chlorthal-dimethyl; Chlozolinate; Coumaphos; Cyanazine; Cyfluthrin (the sum of Cyfluthrin isomers including other compound isomer mixtures); Cyhalofop-butyl; Cypermethrin (the sum of Cypermethrin isomers including other compound isomer mixtures); Dazomet; HCH-delta (Hexachlorocyclohexane- delta); Deltamethrin (cis-deltamethrin); Demeton-S-methyl; Demeton- S- methyl sulfone; Desmetryn; Dialifos (Dialifor); Diazinon; Dichlofluanid; Dichlorvos; Diclofopmethyl; Dicloran; Dicofol; Dicrotophos; Dimethachlor; Dimethipin; Dimethoate; Dinobuton; Disulfoton; Ditalimfos; Endosulfan (the sum of alpha and beta- endosulfan and Endosulfan sulphate , calc. as Endosulfan ); Endrin; EPN; Ethofumesate 2-keto (2,3-dihydro-3,3- dimethyl-2-oxo-benzofuran-5-yl methanesulphonate); Fenvalerate (each ratio of the respective isomers (RR, SS, RS and SR) including Esfenvalerate); Ethalfluralin; Ethion; Ethoprophos; Etridiazole; Etrimfos; Fenamiphos; Fenamiphos sulfone; Fenarimol; Fenchlorphos; Fenhexamid; Fenitrothion; Fenpiclonil; Fenpropathrin; Fenson; Fenthion; Fenthion sulfone; Fenthion sulfoxide; Fipronil; Flucythrinate (the sum of isomers including other mixtures of Flucythrinate isomer compounds); Fluvalinate (the sum of isomers, resulting from the use of tau-fluvalinate); Fluotrimazole; Folpet (the sum of Folpet and Phtalimide , calc. as Folpet ); Fonofos; Formothion; Fosthiazate; Fuberidazole; Gamma cyhalothrin; Heptachlor (the sum of Heptachlor and Heptachlor epoxide, calc. as Heptachlor); Heptenophos; Hexachlorobenzene (HCB); Hexaconazole; Imazalil; Iodofenphos (Jodfenphos); Iprodione; Isazofos; Isodrin; Lambda- cyhalothrin (the sum of R,S and S,R isomers including gamma-cyhalothrin); Lindane (gamma-isomer of Hexachlorocyclohexane (HCH)); Leptophos; Linuron; Malathion (the sum of Malathion and Malaoxon ; calc. as Malathion); Mecarbam; Mephosfolan; Merphos; Methacrifos; Methamidophos; Methidathion; Methoxychlor; Metrafenone; Mevinphos; Molinate; Monocrotophos; Myclobutanil; Naled; Nitrofen; Omethoate; Oxyfluorfen; Paraoxon- ethyl (Paraoxon); Parathion-ethyl (Parathion); Parathion-methyl (the sum of Parathion- methyl and Paraoxon-methyl, calc. as Parathion-methyl); Pebulate (Pebulat); Pendimethalin; Pentachloroaniline; Permethrin (sum of isomers); Phenthoate; Phorate; Phosalone; Phosphamidon; Pirimiphos-ethyl; Pirimiphos-methyl; Procymidone; Propanil; Propyzamide; Prosulfocarb; Prothiophos; Pyrazophos; Pyridaben; Pyridaphenthion; Quinalphos; Chinomethionat (aka quinomethionate); Quintozene (PCNB) (the sum of Quintozene and Pentachloro aniline ; calc.as Quintozene); Spiromesifen; Sulfotep; Sulprofos (Bolstar); Tecnazene; Tefluthrin; Terbacil; Terbufos; Terbufos-sulfone; Terbutryn; Tetrachlorvinphos; Tetraconazole; Tetradifon; Tetrasul; Thiobencarb (Benthiocarb); Thiometon; Tolclofos- methyl; Tolylfluanid (the sum of tolylfluanid and dimethylaminosulfotoluidide, calc.as tolylfluanid); Triadimefon; Triadimenol; Tri-allate; Triazophos; Trifloxystrobin; Trifluralin; Vinclozolin]

AOAC 2007.01

Foods with High Sugar and Low Water Content

Detection and Quantification Analysis of Selected Pesticides

LC-MS/MS Method

[Number of Selected Pesticides Analyzed is 70-

Acetamiprid; Azoxystrobin; Benalaxyl; Bendiocarb; Buprimate; Carbaryl; Carbendazim; Carbofuran; Carboxin; Clothianidin; Desmedipham; Diethofencarb; Dimethanamide; Dioxacarb; Dioxathion; Ethidimuron; Ethiofencarb; Etoxazole; Fenamidone; Fenazaquin; Fenobucarb; Fenpropimorph; Fenproximate; Fensulfothion; Florasulam; Fluazifop-p-butyl; Flufenoxuron; Fluopicolide; Fluquinconazole; Flusilazole; Furalaxyl; Isofenphos; Imidacloprid; Lenacil; Mepronil; Metaflumizone; Metalaxyl; Metazachlor; Metconazole; Methiocarb sulfon; Methoxyfenozide; Metobromuron; Metolachlor; Napropamide; Ofurace; Oxamyl; Oxycarboxin; Paclobutrazol; Pencycuron; Phenmedipham; Phoxim; Pirimicarb; Prochloraz; Promecarb; Propargite; Propazine; Propoxur; Pymetrozine; Pyrifenox; Pyriproxyfen; Rabenzazole; Spiroxamine; Terbumeton; Thiabendazole; Thiacloprid; Thiamethoxam; Tralkoxydim; Tribenuron- methyl; Triflumizole; Vamidothion]

AOAC 2007.01

Eggs

Detection and Quantification Analysis of Selected Pesticides

LC-MS/MS Method

[Number of Selected Pesticides Analyzed is 59-

Acetamiprid; Azoxystrobin; Benalaxyl; Bendiocarb; Buprimate; Carbendazim; Carbofuran; Carboxin; Clothianidin; Desmedipham; Diethofencarb; Dimethanamide; Dimethomorph; Dioxacarb; Dioxathion; Ethidimuron; Ethiofencarb; Etoxazole; Fenamidone; Fenobucarb; Fensulfothion; Fipronil; Fipronil sulfone; Florasulam; Fluazifop-p-butyl; Flufenoxuron; Fluopicolide; Foramsulfuron; Furalaxyl; Imidacloprid; Isofenphos; Isoproturon; Metaflumizone; Metalaxyl; Metazachlor; Metconazole; Methomyl; Metobromuron; Oxamyl; Oxycarboxin; Paclobutrazol; Pencycuron; Phosmet; Phoxim; Pirimicarb; Promecarb; Propargite; Propazine; Prosulfuron; Pymetrozine; Pyrifenox; Pyriproxyfen; Terbumeton; Terbuthylazine; Thiabendazole; Thiacloprid; Thiamethoxam; Triflumizole; Vamidothion]

AOAC 2007.01

Foods with High Water Content, and Foods with High Acid and High Water Content

Detection and Quantification Analysis of Selected Pesticides

LC-MS/MS Method

[Number of Selected Pesticides Analyzed is 405

2,4 DNOP (Meptyldinocap-phenol); 2,4 DNOPC (Meptyldinocap); 2,4,6-Trichlorophenol; 2,4-DB; 2,4-D (2,4- Dichlorophenoxyacetic acid); 2- Hydroxy-propoxycarbazone; 4,6-dihydroxy tembotrione; 6-Benzyladenine; 8- hydroxyquinoline (Quinolinol); Abamectin (the sum of Avermectin (B1a)- Avermectin (B1b)mix); Acephate; Acequinocyl; Acetamiprid; Acibenzolar acid (CGA 210007); Acrinathrin; Aldicarb (the sum of Aldicarb sulfoxide and Aldicarb sulfone, calc. as Aldicarb); Ametoctradin; Amidosulfuron; Aminopyralid; Amitraz (including its metabolites containing the 2,4-dimethylaniline group, in terms of Amitraz); Anilofos; Atrazine; Azadirachtin; Azimsulfuron; Azinphos methyl; Aziprotryne; Azoxystrobin; Benalaxyl; Bendiocarb; Bensulfuron-methyl; Bentazone; Bentazone-6-hydroxy; Bentazone-8-hydroxy; Benzobicyclon; Bicyclopyrone metabolite (CSCD686480); Bicyclopyrone metabolite (SYN503780); Bifenazate (sum of bifenazate plus bifenazate-diazene expressed as bifenazate); Bispyribac sodium; Bitertanol; Bixafen; Boscalid; Bromacil; Bromoxynil; Bromuconazole; Bupirimate; Buprofezin; Butralin; Butylate; Cadusafos; Carbaryl; Carbendazim and Benomyl (the sum of Benomyl and Carbendazim, calc. as Carbendazim); Carbofuran (all Carbofuran produced from Carbosulfan, Benfuracarb or Furathiocarb and the sum of 3-OH Carbofuran in terms of Carbofuran); Carboxin (sum of carboxin and its metabolites carboxin sulfoxide and oxycarboxin (carboxin sulfone), calc. as carboxin); Carfentrazone-ethyl; Chlorantraniliprole; Chlorbromuron; Chlorfenvinphos; Chlorfluazuron; Chlorfluazuron; Chloridazon ( the sum of Chloridazon and Chloridazon-desphenyl, calc. as Chloridazon); Chlorotoluron; Chloroxuron; Chlorpyrifos; Chlorsulfuron; Clethodim (Total of Sethoxydim and Clethodim, including cleavage products calc. as Sethoxydim); Clodinafop (free acid); Clodinafop-propargyl; Clofentezine; Clomazone; Clothianidin; Coumaphos; Cyanazine; Cyazofamid; Cycanilide; Cycloate; Cycloxydim; Cyflufenamid; Cyflumetofen; Cymoxanil; Cyproconazole; Cyprodinil; Cyromazine; Deltamethrin (cis-deltamethrin); Demeton S methyl; Demeton S methyl sulfone; Desmedipham; Diafenthiuron; Diazinon; Dicamba; Dichlorprop; Dichlorprop-P; Dichlorvos; Dicrotophos; Diethofencarb; Difenoconazole; Diflubenzuron; Diflufenican; Dimefox; Dimethachlor; Dimethenamide (sum of isomers containing other mixtures of component isomers including dimethenamide-P); Dimethoate; Dimethomorph (sum of isomers); Diniconazole (sum of isomers); Dinocap; Dinoseb; Dioxacarb; Dioxathion; Diphenamid; Diphenylamine; Disulfoton (the sum of Disulfoton, Disulfoton sulfoxide and Disulfoton sulfone; calc. as Disulfoton); Ditalimfos; Dithianon; Diuron; DNOC; Dodine; Emamectin benzoate B1a (in terms of Emamectin); Epoxiconazole; EPTC (ethyl dipropylthiocarbamate); Ethametsulfuron methyl; Ethidimuron; Ethiofencarb; Ethion; Ethirimol; Ethofumesate (the sum of Ethofumesate and metabolite 2,3-dihydro-3,3- dimethyl-2-oxo-benzofuran-5-yl methanesulphonate); Ethoprophos; Ethoxyquin; Ethoxysulfuron; Etofenprox; Etoxazole; Etrimfos; Famoxadone; Fenamidone; Fenamiphos; Fenamiphos sulfone; Fenamiphos sulfoxide; Fenazaquin; Fenbuconazole (component isomers); Fenhexamid; Fenobucarb; Fenoxaprop-P; Fenoxaprop-P-ethyl; Fenoxycarb; Fenpropathrin; Fenpropidin; Fenpropimorph (sum of isomers); Fenpyrazamine; Fenpyroximate; Fensulfothion; Fenthion; Fenthion oxon; Fenthion oxon sulfoxide; Fenthion sulfoxide; Fentin acetate; Fipronil (the sum of fipronil and sulfone metabolite (MB46136); calc. As Fipronil ); Flazasulfuron; Flonicamid; Florasulam; Florpyrauxifen benzyl; Fluazifop-P; Fluazifop-P-butyl; Fluazinam; Flubendiamide; Flucarbazone sodium; Fludioxonil; Flufenacet; Flufenacet ethane sulfonic acid (ESA) sodium salt; Flufenoxuron; Flufenzin; Fluometuron; Fluopicolide; Fluopyram; Fluoxastrobin (Fluoxastrobin ve Z-izomer toplamı); Flupyradifurone; Fluquinconazole; Flurochloridone (sum of cis- and trans- isomers); Fluroxypyr; Fluroxypyr-1-methylheptyl ester; Fluroxypyr-2-methoxy; Flusilazole; Fluthiacet methyl; Flutolanil; Flutriafol; Fluxapyroxad; Fomesafen; Fonofos; Foramsulfuron; Forchlorfenuron; Formetanate; Fosthiazate; Fuberidazole; Furalaxyl; Halauxifen methyl (halauxifen methyl ve X11393729 (halauxifen) toplamı, halauxifen-methyl cinsinden); Halosulfuron methyl; Haloxyfop; Haloxyfop (free acid); Haloxyfop-2-etoxy ethyl; Haloxyfop-R-methyl; Heptenophos; Hexaconazole; Hexaflumuron; Hexythiazox; Hymexazol; IM-2- 1(Acetamiprid-N-desmethyl); Imazalil; Imazamox; Imazapic; Imazapyr; Imazethapyr; Imidacloprid; Indaziflam; Indole 3-butyric acid; Indoxacarb; Iodosulfuron methyl; Iodosulfuron-methyl-sodium; Ioxynil; Ipconazole; Iprodione; Iprovalicarb; Isazofos; Isocarbophos; Isofenphos; Isofenphos-methyl; Isoprocarb; Isoproturon; Isopyrazam; Isoxaben; Isoxaflutole; Kresoxim-methyl; Lenacil; Linuron; Lufenuron (Any ratio of component isomers); Malathion (the sum ofMalathion and Malaoxon; calc. as Malathion); Mandipropamid (any ratio of component isomers); MCPA; MCPB; Mecarbam; Mecoprop (the sum of Mecoprop-P and Mecoprop ; calc. as Mecoprop); Mefenpyr-diethyl; Mefentrifluconazole; Mepanipyrim; Mepronil; Mesosulfuron methyl; Mesotrione; Metaflumizone; Metalaxyl and Metalaxyl-M (the sum of Metalaxyl isomers along with other compound isomer mixtures including Metalaxyl-M); Metamitron; Metazachlor; Metazachlor 479M08; Metconazole (sum of isomers); Methamidophos; Methidathion; Methiocarb (Methiocarb and the sum of Methiocarb sulfoxide and sulfone; calc. as in Methiocarb); Methomyl; Methoprene; Methoxyfenozide; Metobromuron; Metolachlor and S-Metolachlor (sum of isomers including S-metolachlor and related other components); Metolachlor-S; Metosulam; Metoxuron; Metrafenone; Metribuzin; Metsulfuron-methyl; Mevinphos; Monocrotophos; Monolinuron; Myclobutanil; Napropamide (sum of isomers); Nicosulfuron; Norflurazon; Novaluron; Nuarimol; Ofurace; Orthosulfamuron; Oxadiazon; Oxadixyl; Oxamyl; Paclobutrazol (sum of component isomers); Penconazole (sum of component isomers); Paraoxon ethyl; Parathion methyl (the sum of Parathion methyl and Paraoxon methyl, calc. as Parathion methyl); Penconazole; Pencycuron (the sum of pencycuron and pencycuron-PB-amine, calc. as pencycuron); Pendimethalin; Penflufen; Penoxsulam; Pentanochlor; Penthiopyrad; Phenmedipham; Phenthoate; Phorate sulfone; Phosalone; Phosmet; Phosmet oxon; Phosphamidon; Phoxim; Picloram; Picoxystrobin; Pinoxaden; Pirimicarb (the sum of Pirimicarb and desmethyl pirimicarb; calc. as Pirimicarb); Pirimiphos ethyl; Pirimiphos methyl; Primisulfuron- methyl; Prochloraz; Prochloraz desimidazole-amino; Profenofos;Profoxydim-lithium; Promecarb; Prometryn; Propachlor; Propamocarb; Propaquizafop; Propargite; Propazine; Propham; Propiconazole (sum of isomers); Propoxur; Propoxycarbazone; Propoxycarbazone sodium; Propyzamide; Proquinazid; Prosulfocarb; Prosulfuron; Prothioconazole; PTU (propylene thiourea); Pymetrozine; Pyraclostrobin; Pyraflufen-ethyl; Pyrazophos; Pyrethrins; Pyridaben; Pyridafol; Pyridalyl; Pyridalyl; Pyridaphention; Pyridate; Pyrifenox; Pyrimethanil;Pyriofenone; Pyriproxyfen; Pyroxsulam; Quinalphos; Quinclorac; Quinmerac; Quinoxyfen; Quizalofop; Quizalofop free acid; Quizalofop-P tefuryl; Quizalofop-P-ethyl; Rabenzazole; Rimsulfuron; Sedaxane (izomerler toplamı); Simazine; Sodium 5- nitroguaiacolate, sodium o-nitrophenolate ve sodium p-nitrophenolate toplamı, sodium 5-nitroguaiacolate cinsinden; Spinetoram (Spinetoram-J ve Spinetoram-L toplamı); Spinosad; Spirodiclofen; Spirotetramat ve spirotetramat- enol toplamı, spirotetramat cinsinden; Spiroxamine (sum of isomers); Sulfosulfuron; Sulfotep; Tebuconazole; Tebufenozide; Tebufenpyrad; Teflubenzuron; Tembotrione (ana tembotrione (AE0172747) ve metabolit M5 (4,6- dihydroxy tembotrione) toplamı, tembotrione cinsinden); Tepraloxydim; Terbumeton; Terbuthylazine; Tetrachlorvinphos; Tetraconazole; Tetramethrin; TFNA; TFNG; Thiabendazole; Thiacloprid; Thiamethoxam; Thiencarbazone methyl; Thifensulfuron-methyl; Thiodicarb; Thiophanate-methyl; Tolfenpyrad; Tralkoxydim (sum of component isomers); Triadimefon; Triadimenol; Triasulfuron; Triazophos; Tribenuron-methyl; Trichlorfon; Triclopyr; Triclopyr-2-butoxyethyl ester; Tridemorph; Trifloxystrobin; Trifloxysulfuron; Triflumizole; Triflumuron; Triflusulfuron (6-(2,2,2- trifluoroethoxy)-1,3,5-triazine-2,4-diamine (IN-M7222); Triforine; Trinexapac (free acid); Trinexapac ethyl; Triticonazole; Tritosulfuron; Valifenalate; Vamidothion; Vernolate; Zoxamide]

AOAC 2007.01

Food (not applicable to tea and coffee)

Determination of Caffeine

HPLC-UV/DAD Method

JAOAC Vol.76 No:2

Food

Determination of Acesulfame K, Saccarin, Aspartame

HPLC-UV/DAD Method

JAOAC Vol.76 No:2

Food

Determination of Benzoic Acid and Sorbic Acid

HPLC-UV/DAD Method

NMKL 124

Vegetables

Analysis of Nitrate

HPLC-UV/DAD Method

JAOAC Vol.76 No 2

Sugary Products

Determination of HMF

HPLC-UV/DAD Method

JAOAC Vol.76 No 2

Nuts and Products

Determination of Aflatoxin B1 and Total Aflatoxin (B1+B2+G1+G2)

HPLC-FLD Method

AOAC 991.31

Feed

Determination of Aflatoxin B1 and Total Aflatoxin (B1+B2+G1+G2)

HPLC-FLD Method

In-house Method- “KMB-TL-07 Rev. No:01” (Modified from R-Biopharm Application Note; Ref No: A13- P07.V6 )

Spices

Determination of Aflatoxin B1 and Total Aflatoxin (B1+B2+G1+G2)

HPLC-FLD Method

In-house Method-“KMB-TL-08 Rev. No:00” (Modified from R-Biopharm Application Note A17-P07.V6 )

Cereals

Determination of Aflatoxin B1 and Total Aflatoxin (B1+B2+G1+G2)

HPLC-FLD Method

In-house Method- “KMB-TL-06 Rev. No:00” (Modified from R-Biopharm Application Note; Ref No: RP71- A1.V4 )

Dried Fig and Fig Products

Determination of Aflatoxin B1 and Total Aflatoxin (B1+B2+G1+G2)

HPLC-FLD Method

TS EN 14123

Milk; Milk powder

Determination of Aflatoxin M1

HPLC-FLD Method

In-house Method- “KMB-TL-25 Rev. No:01”(Modified from R-Biopharm Application Note; Ref No: A11-RP 71/70N.V3)

Dried Fruits

Determination of Ochratoxin A

HPLC-FLD Method

In-house Method  “KMB-TL-22  Rev. No:00” (Modified from R-Biopharm Application Note Ref No: A8 -P14.V6)

Coffee

Determination of Ochratoxin A

HPLC-FLD Method

In-house Method-”KMB-TL-28 Rev. No:01” (R-Biopharm Okraprep Application Note; Ref No: A1-P14.V9)

Cereals, Grain-Based Food and Feed

Determination of Deoxynivalenol (DON)

HPLC-UV/DAD Method

In-house Method- “KMB-TL-26 Rev. No:01” (Modified from R-Biopharm Application Note; Ref No: RP50/V8/26.10.10)

Cereals, Grain-Based Food and Feed

Determination of Zearelonone (ZON)

HPLC-FLD Method

In-house Method-“KMB-TL-27 Rev. No:00” (Modified from R-Biopharm Application Note; Ref No: RP91/V12/26.10.1)

Food and Feed (Cereal and Grain-based Food and Feed)

Determination of Multiple Mycotoxin [Aflatoxin B1; B2; G1; G2; Ochratoxin A; Zearalenone; Deoxynivalenol; T-2 Toxin; HT-2 Toxin; Fumonisin (FB1 +FB2)]

LC-MS/MS Method

In-house Method-“KMB-TL-04 Rev. No:00”(Modified from ANT Teknik Application Note, Multitoxin Analysis in Foods by LC-MS/MS and M016/2015 Application Notes)

Food

Determination of Multiple Mycotoxin Aflatoxin (B1;B2;G1;G2, Ochratoxin A)

LC-MS/MS Method

In-house Method- “KMB-TL-10”, Rev:00” (Modified from ANT Teknik Application Note, Multitoxin Analysis in Foods by LC-MS/MS and M016/2015 Application Notes)

Seafood

Determination of Polycyclic Aromatic Hydrocarbons (PAH) [Benzo (a) pyrene

Pre-Treatment: Liquid-Liquid Extraction

Measurement: HPLC UV/FLD Method

In-house Method-“ KMB-TL-87 Rev. No 00” (Modified from Agilent 5990-5441EN, 2010 application note)

Food

Analysis of Aluminum (Al), Arsenic (As), Copper (Cu), Mercury (Hg), Zinc (Zn), Iron (Fe), Cadmium (Cd), Tin (Sn), Calcium (Ca), Lead (Pb), Magnesium (Mg), Potassium (K), Sodium (Na)

ICP-MS Method

NMKL 186

Plastic Materials and Articles in Contact with Foodstuffs

Analysis of Total Migration in Evaporable Food Simulants

TS EN 1186-3:2022

Metot 1 (Total Immersion)

Metot 2  (Cell)

Metot 3 (Fillable Pouch)

Metot 4 (Reverse Pouch)

 Metot 5 (Fiilling a Container)

Plastic materials and materials in contact with food

Structure Analysis

FT-IR (Fourier Transform Infrared Spectroscopy) Method

In-house Method-“ALB-TL-06 Rev. No:01” Modified from: (-BIO-RAD Sadtler Spectral Databases Library Polymers Vol.2 -Perkin Elmer FTIR Spectrum Two Handbook. - Anonymous, 1999. Polymer Data Handbook, Modified from Oxford University Press)

Plastic materials and materials in contact with food

Phthalates Analysis

[Number of Parameters - 8]

(BBP/ Butylbenzylphthalate,

DBP/ Dibutylphthalate,

DEHP/ Di-(2-ethylhexyl) phthalate,

DIDP/ Di-isodecylphthalate,

DINP/ Di-iso-nonylphthalate,

DNOP/ Di-n-octyl phthalate,

DIBP/ Diisobutyl phthalate,

DEP/ Diethyl phthalate)

GC-MS Method

In-house Method-“ALB-TL-19 Rev. No:03” Modified from: (-EN 13130-1 -EUR 24387 EN 2010 -EUR 23972 EN 2009 -EUR 24105 EN-1st edition 2009 –EN 14372:2004)

Food (not applicable to dried onions, leeks, and cabbage)

Determination of Sulfur dioxide (SO2)

Titrimetric method

AOAC 962.16

Honey

Determination of Glucose, Fructose,

Ratio of Fructose/Glucose,

Total of Fructose+Glucose

HPLC-RID Method

AOAC 979.23

Honey

Determination of Sucrose and Maltose

HPLC- RID Method

AOAC 977.20

Honey

Determination of Diastase Activity

Spectrophotometric Method

IHC Phadebas Diastase Determination Method

Honey

Electrical Conductivity

TS 13366

Honey

Determination of Free acidity

TS 13360

Honey

Water Content and Refractive Index

TS 13365

Honey

Determination of Proline

Spectrophotometric method

IHC 2009

Fruit-Vegetables and Products

Determination of Brix (Solids Soluble in Water)

Refractometric Method

AOAC 932.14

TS ISO 2173

Tomato paste

Determination of Color

TS 1466

Spices

Determination of Moisture

Toluene Method

TS ISO 939

Products Based-on Plant Origin (Excluding Spices)

Determination of Moisture

TS EN ISO 712-1

Fruit-Vegetables and Products

Determination of Moisture

TS 1129 ISO 1026

Black tea

Determination of Moisture

TS 1562

Cocoa (ground)

Determination of Moisture

TS 3076-1

Instant Dry Soup Mix

Determination of Moisture

TS 3190

Legumes

Determination of Moisture

TS ISO 24557

Oil seeds

Determination of Moisture

TS EN ISO 665

Starch

Determination of Moisture

TS 1252 EN ISO 1666

Sugars for Human Consumption

Determination of Moisture

Turkish Food Codex (TFC) Communiqué No: 2002/26 RG:10.04.2002-24722

Grains and Grain Products (Except Corn and Legumes)

Determination of Moisture

TS EN ISO 712-1

Spices, Seasonings and Medicinal Plants

Essential oil analysis

TS EN ISO 6571

Cereals, Legumes and Byproducts (excluding Starches and Their Products)

Determination of Ash

TS EN ISO 2171

Black Tea

Determination of Total Ash

TS 1564

Spices and Flavoring Agents

Ash determination

TS 2131 ISO 928

Products Based-on Plant Origin

Determination of Starch

Polarimetric Method

TS EN ISO 10520

Fruit and Vegetable Products

Determination of titratable acidity

TS 1125 ISO 750

Fruit and Vegetable Products

Determination of pH

Potentiometric method

TS 1728

ISO 1842

Products Based-on Plant Origin

Determination of Salt

Potentiometric method

AOAC 971.27

Products Based on Plant Origin

Determination of Salt

Titrimetric Method

TS 5000

TS 774

Products Based-on Plant Origin

Determination of Crude Protein

Combustion Method (The principle of Dumas)

AOAC 990.03

Products Based-on Plant Origin

Determination of Fat Content

TS EN ISO 659

TS 2664

Products Based-on Plant Origin

Total Carbohydrate Calculation

TS EN ISO 10520

AOAC 968.28

Products Based-on Plant Origin

Determination of Total Sugar; Invert Sugar; Sucrose

Lane-Eynon Method

TS 1466

Fruit and vegetable products and sugary products

Determination of Sugar Composition (Fructose, Glucose, Sucrose, Maltose)

Ratio of Fructose/Glucose,

Total of Fructose+Glucose

HPLC-RID Method

AOAC 977.20

AOAC 980.13

Herbal product compositions,  food supplements, energy drinks, herbal tea, coffee, soft drinks, plant extracts, paste, honey, chocolate, Turkish delight, cezerye etc. other sugary products

Analysis of some selected drug active ingredients/active pharmaceutical ingredients

Number of Selected Pesticides Analyzed is 110

2,4-dinitrofenol (2,4-dinitrophenol (DNP), (2,4-DNP)), 6-α-metilprednizolon (6-α-methylprednisolone), Amfetamin (Amphetamine), Amlodipin (Amlodipine), Asetildenafil (Acetildenafil), Atorvastatin (Atorvastatin Calcium Salt), Atropin (Atropine), Avanafil (Avanafil), Benazepril, Benzil Sibutramin (Benzyl Sibutramine HCl), Benzil Sildenafil (Benzyl Sildenafil), Betametazon (Betamethasone), D,L-Venlafaksin (D,L-Venlafaxine Hydrochloride), Dapoksetin (Dapoxetine Hydrochloride), Dekzametazon (Dexamethasone), Desmetil Sibutramin (Desmethyl Sibutramine), 1Didesmetil Sibutramin (Didesmethyl Sibutramine), Digitoksin (Digitoxin), Diklofenak (Diclofenac), Dimetil Sildenafil (Dimethyl Sildenafil), Dobutamin (Dobutamine), Efedrin (Ephedrine), Enalapril, Felodipin (Felodipine), Fenasetin (Phenacetin), Fenformin (Phenformin), Fenilbutazon (Phenylbutazone), Fentolamin (Phentolamine), Finasterid (Finasterid), Fluoksetin (Fluoxetine Hydrochloride), Fluvastatin (Fluvastatin Sodium Salt), Fluvoksamin (Fluvoxamine), Fondenafil (Fondenafil), Furosemit (Furosemide), Glibenklamid (Glibenclamide), Gliklazid (Gliclazide), Glimepirid (Glimepiride), Glipizid (Glipizide), Hidralazin (Hydralazine), Hidroklorothiazit (Hydrochlorothiazide), Hidroksi Klorodenafil (Hydroxy Chlorodenafil), Hidroksihomosildenafil (Hydroxyhomo Sildenafil), Hidroksithiohomo Sildenafil (Hydroxythiohomo Sildenafil), Homo Sibutramin (Homo Sibutramine HCl), Homo Sildenafil, İbuprofen (Ibuprophen), İndometazin (Indomethacin), Kannabidiol (Cannabidiol), Kannabigerol (Cannabigerol), Kannabinol (Cannabinol), Kannobidiolik Asid (Cannobidiolic Asid), Kaptopril (Captopril), Karvedilol (Carvedilol), Ketoprofen, Kinidin (Quinidine), Klenbuterol Hidroklorit (Clenbuterol Hydrochloride), Klonidin (Clonidine), Klorfeniramin Maleat (Chlorpheniramine Maleate), Kloro-Sibutramin (Chloro-Sibutramine HCl), Klortalidon (Chlorthalidone), Labetalol, Lisinopril, Lovastatin (Lovastatine), Mefenamik Asit (Mefenamic Acid), Metamizol (Metamyzole), Metformin, Metoprolol, Mevastatin (Mevastatine), Minoksidil (Minoxidil), N,N-didemeti 1-Hidroksi Sibutramin (N,N-didemethyl 1-Hydroxy Sibutramine Hydrochloride), Naproksen (Naproxen), Natamisin (Natamycin), Nifedipin (Nifedipine), Nitrendipin (Nitrendipine), Nitrodenafil (Nitrodenafil), Norpsödoefedrin (Norpseudoephedrine), Omeprazol (Omeprazole), Parasetamol (Paracetamol), Paroksetin (Paroxetine Hydrochloride), Pitavastatin (Pitavastatin Calcium), Prazosin, Prednizolon (Prednisolone), Propoksifenil Homohidroksi Sildenafil (Propoxyphenyl Homohydroxy Sildenafil), Propoksifenil tiyohidroksihomo Sildenafil (Propoxyphenyl-thiohydroxyhomo Sildenafil), Psödoefedrin (Pseudoephedrine), Ramipril, Repaglinid (Repaglinide), Rosiglitazon (Rosiglitazone), Rosuvastatin (Rosuvastatin Calcium Salt), Sertralin (Sertraline Hydrochloride), Sibutramin (Sibutramine), Sildenafil, Sildenafil Amid (Sildenafil Amid), Simvastatin (Simvastatine), Sitalopram (Citalopram), Skopolamin (Scopolamine), Tadalafil ,Tetra Hidro Kannobinol (Tetra Hydro Cannobinol), Tetra Hidro Kannobinolik Asid (Tetra Hydro Cannobinolic Asid), Thiodimetilsildenafil (Thiodimethyl Sildenafil), ThiohomoSildenafil, Thiosildenafil, Tolbutamid (Tolbutamide), Triamsinolon Asetonit (Triamcinolone Acetonide), Triamteren (Triamterene), Valsartan, Vardenafil, Verapamil, Yohimbin (Yohimbine), Zimeldin (Zimeldine)

In House Method “BÜB-TL-220 Rev. No 01” (Modified from Journal of Pharmaceutical and Biomedical Analysis 41 (2006) 554-564)

Vegetable oils

Determination of Fatty Acid Composition

(Arachidic acid (C20:0); Behenic acid (C22:0); Heptadecenoic acid (cis-10) (C17:1); Gadoleic acid (C20:1); Erucic acid (C22:1); Margaric acid (C17:0); Lauric asit (C12:0); Lignoceric acid (C24:0); Linoleic acid (C18:2); Linolenic acid (C18:3); Myristic acid (C14:0); Oleic acid (C18:1); Palmitic acid (C16:0); Palmitoleic acid (C16:1); Stearic acid (C18:0))

GC-FID Method

Com. Regulation (EC) No 796

COI/T.20/Doc. No 33

Vegetable oils

Determination of Peroxide Value

TS EN ISO 3960

Vegetable Oils

Determination of Refractive Index

TS EN ISO 6320

Vegetable oils

Determination of Free Fatty Acidity /Acid Number

TS 894

TS EN ISO 660

Extra Virgin Olive

Oil

Sensory Analysis

Turkish Food Codex Olive Oil And Pomace Oil Analysis Methods Notification (Notification No: 2023/20) COI/T.20/Doc. No 15 Determination of Sensory Properties of Natural Olive Oils (Except for articles 4.4 and 10.4)

Cheese

Determination of Total Dry Matter

TS EN ISO 5534

Cheese

Determination of Salt Content

Mohr Method

In-house Method-“ HÜB-TL-159/01 Rev. No 07”, (Modified from Food Inspection Analysis Methods, 1988)

Cheese

Determination of Fat Content

Van Gulik Method

TS ISO 3433

Cheese

Determination of Acidity

TS 591

Yogurt

Determination of Fat

TS 1330

Milk, Ayran, Cream and Condensed Milk

Determination of Dry Matter

TS 1018

Yogurt

Determination of Dry Matter / Moisture

In House Method-“ HÜB-TL-71/01 Rev. No 09 (Modified from GMMAM)

Butter

Determination of Dry Matter / Moisture

TS 1331

Raw milk

Determination of Phosphatase Activity

Lactognost Assay Method;

In House Method-“HÜB-TL-90/01 Rev. No:04” (Modified from Lactognost Test Kit Application Note, Heyl)

Milk and dairy products

Determination of Lactose

Lane-Eynon Method

In House Method-“HÜB-TL-105/01 Rev. No:02”(Modified from Food Inspection Analysis Methods, 1988)

Milk and ayran

Determination of Acidity

TS 1018

Milk and ayran

Determination of Fat

AOAC 2000.18

Butter

Determination of Salt Content

Mohr Method

In House Method-“HÜB-TL-159/01 Rev. No 07”, (Modified from Food Inspection Analysis Methods, 1988)

Milk and dairy products

Determination of Total Protein

AOAC 991.20

TS EN ISO 8968-1

Seafood

Determination of Histamine

HPLC-UV/DAD method

NMKL 196

Milk and dairy products

Species Identification (Detection of Bovine DNA)

Real Time-PCR Method

Pretreatment: DNA Extraction

Kit Method (SNPRTs-SG Milk Specimen Panel Kit Procedure)

Kit Method (NucleoSpin Genomic DNA extraction kit procedure)

Milk and dairy products

Species Identification (Detection of Sheep DNA)

RealTime-PCR Method

Pretreatment: DNA Extraction

Kit Metodu (SNPRTs-KY Milk Specimen Panel Kit Procedure)

Kit Method (NucleoSpin Genomic DNA extraction kit procedure)

Milk and dairy products

Species Identification (Detection of Goat DNA)

RealTime-PCR Method

Pretreatment: DNA Extraction

Kit Metodu (SNPRTs-KÇ Milk Specimen Panel Kit Procedure) Kit Method

(NucleoSpin Genomic DNA extraction kit procedure)

Meat; Meat Products and Dairy Products

Species Identification (Detection of Horse DNA)

Real Time PCR Method

Pretreatment: DNA Extraction

Kit Metodu (SNPRT-A Speciation Panel Kit Procedure) Kit Method (NucleoSpin Genomic  DNA extraction kit procedure)

Meat; Meat Products and Dairy Products

Species Identification (Detection of Donkey DNA)

Real Time PCR Method

Pretreatment: DNA Extraction

Kit Metodu (SNPRT-E Speciation Panel Kit Procedure)

Kit Method (NucleoSpin Genomic DNA extraction kit procedure)

Meat; Meat Products and Dairy Products

Species Identification (Detection of Pig DNA)

Real Time PCR Method

Pretreatment: DNA Extraction

Kit Metodu (SNPRT- D, Speciation Panel Kit Procedure)

Kit Method (NucleoSpin Genomic DNA extraction kit procedure)

Meat; Meat Products and Dairy Products

Species Identification (Detection of Chicken DNA) 

Real Time PCR Method

Pretreatment: DNA Extraction

Kit Metodu (SNPRT- T Speciation Panel Kit Procedure)

Kit Method (NucleoSpin Genomic DNA extraction kit procedure)

Meat; Meat Products and Dairy Products

Species Identification (Detection of Turkey DNA

Real Time PCR Method

Pretreatment: DNA Extraction

Kit Metodu (SNPRT-H Speciation Panel Kit Procedure)

Kit Method (NucleoSpin Genomic DNA extraction kit procedure)

Meat; Meat Products and Dairy Products

Species Identification (Detection of Beef DNA)

Real Time PCR Method

Pretreatment: DNA Extraction

Kit Metodu (SNPRT- SG Speciation Panel Kit Procedure)

Kit Method (NucleoSpin Genomic DNA extraction kit procedure)

Meat; Meat Products and Dairy Products

Species Identification (Detection of Sheep DNA)

Real Time PCR Method

Pretreatment: DNA Extraction

Kit Metodu (SNPRT- KY Speciation Panel Kit Procedure)

Kit Method (NucleoSpin Genomic DNA extraction kit procedure)

Meat; Meat Products and Dairy Products

Species Identification (Detection of Goat DNA)

Real Time PCR Method

Pretreatment: DNA Extraction

Kit Metodu (SNPRT-KÇ Speciation Panel Kit Procedure)

Kit Method (NucleoSpin Genomic DNA extraction kit procedure)

Meat; Meat Products and Dairy Products

Species Identification (Detection of Corn DNA)

Real Time PCR Method

Pretreatment: DNA Extraction

Kit Metodu (SNPRT-M Speciation Panel Kit Procedure)

Kit Method (NucleoSpin Genomic DNA extraction kit procedure)

Meat; Meat Products and Dairy Products

Species Identification (Detection of Soybean DNA)

Real Time PCR Method

Pretreatment: DNA Extraction

Kit Metodu (SNPRT-SY Speciation Panel Kit Procedure)

Kit Method (NucleoSpin Genomic DNA extraction kit procedure)

Feed and raw materials of feed

Species Identification (Detection of Bonito DNA)

Real Time PCR Method

Pretreatment: DNA extraction

Kit Metodu (SNP Biotechnology SNPRTB- P, Kit Procedure)

Kit method (nucleospin genomic DNA extraction kit procedure)

Feed and raw materials of feed

Species Identification (Detection of Salmon DNA)

Real Time PCR Method

Pretreatment: DNA extraction

Kit Metodu (SNP Biotechnology SNPRTB-S Kit Procedure)

Kit method (nucleospin genomic DNA extraction kit procedure)

Feed and raw materials of feed

Species Identification (Detection of Sea Bass DNA)

Real Time PCR Method

Pretreatment: DNA extraction

Kit Metodu (SNP Biotechnology SNPRTB-L Kit Procedure)

Kit method (nucleospin genomic DNA extraction kit procedure)

Feed and raw materials of feed

Species Identification (Detection of Anchovy DNA)

Real Time PCR Method

Pretreatment: DNA extraction

Kit Metodu (SNP Biotechnology SNPRTB- H Kit Procedure)

Kit method (nucleospin genomic DNA extraction kit procedure)

Feed and raw materials of feed

Species Identification (Detection of Sea Bream DNA)

Real Time PCR Method

Pretreatment: DNA extraction

Kit Metodu (SNP Biotechnology SNPRTB-C Kit Procedure)

Kit method (nucleospin genomic DNA extraction kit procedure)

Feed and Feed Additives

Analysis of Selected Veterinary Drug Residues-

LC-MS/MS Method

Amphenicols-3

Chloramphenicol; Florfenicol; Thiamphenicol

Anticoccidials -12

Amprolium; Diclazuril; Halofuginone; Lasalocid; Maduramicin; Monensin; Narasin; Nicarbazin; Robenidine; Salinomycin; Toltrazuril, Decoquinate

Diaminopyrimidines –1

Trimethoprim

Quinolones -6

Ciprofloxacin; Danofloxacin; Difloxacin; Enrofloxacin; Flumequin; Sarafloxacin

Lincosamides -1

Lincomycin

Macrolides-5

Erythromycin; Spiramycin; Tilmicosin Tylosin; Tylvalosin

Nitrofurans-2

Furaltadone; Furazolidone

Penicillins-6

Amoxicillin; Ampicillin; Dicloxacillin; Nafcillin; Oxacillin; Penicillin G

Pleuromutilins-1

Tiamulin

Quinoxalines-2

Carbadox; Olaquindox

Streptogramins-1

Virginamycin

Sulfanamides-10

Sulfachloropyridazine; Sulfadiazine; Sulfadimethoxine; Sulfadoxine; Sulfamerazine; Sulfamethazine; Sulfamethoxazole; Sulfapyridine; Sulfaquinoxaline; Sulfathiazole

Tetracyclines -4

Chlortetracycline; Doxycycline; Oxytetracycline; Tetracycline

In house Method “VKB-TL-01 Rev. No:02” (Modified from: Analytica Chimica Acta 700 (2011) 26-33 and AOAC 997.04)

Milk

Analysis of Selected Veterinary Drug Residues-

LC-MS/MS Method

Amphenicols -3

Chloramphenicol; Florfenicol; Thiamphenicol

Anthelmintics -3

Levamisol; Thiabendazole 5 Hydroxy; Thiabendazole

Quinolones -9

Ciprofloxacin; Danofloxacin; Difloxacin; Enrofloxacin; Flumequin; Marbofloxacin; Nalidixic Acid; Oxolinic Acid; Sarafloxacin

Macrolides -5

Spiramycin; Tilmicosin; Neospiramycin; Tylosin; Erytromycin

Nitrofurans -4

Nitrofurantoin (AHD); Furaldaton (AMOZ); Furazolidon (AOZ); Nitrofurazon (SEM)

Nitroimidazoles -7

Dimetridazole; Ipronidazole Hyrodxy; Ipronidazole; Metronidazole; Ronidazole; HMMNI; Metronidazole Hydroxy

Sulfanamides -10

Sulfachloropyridazine; Sulfadiazine; Sulfadimethoxine; Sulfadoxine; Sulfamerazine; Sulfamethazine; Sulfamethoxazole; Sulfapyridine; Sulfaquinoxaline; Sulfathiazole

Tetracyclines -7

Chlortetracycline; Doxycycline; Oxytetracycline; Tetracycline; 4-epi-Tetracycline; 4-epi-Oxytetracycline; 4-epi-Chlortetracycline

Linkozamid -1

Lincomycin

Penicillin 4

Dicloxacillin; Ampicillin; Cloxacillin; Oxacillin

Beta-lactam -1

Cefquinome (CFQ)

Lincosamide-1

Lincomycin

Macrolides - 5

Erythromycin; Spiramycin; Tilmicosin; Tylosin; Tylvalosin

Nitrofurans -3

Furaltadone; Furazolidone; Nitrofurantoin

Penicillins -3

Amoxicillin; Dicloxacillin; Penicillin G

Pleuromutilins -1

Tiamulin

Quinoxalines -2

Carbadox; Olaquindox

Streptogramins -1

Virginamycin

Sulfanamides -10

Sulfachloropyridazine; Sulfadiazine; Sulfadimethoxine; Sulfadoxine; Sulfamerazine; Sulfamethazine; Sulfamethoxazole; Sulfapyridine; Sulfaquinoxaline; Sulfathiazole

Tetracyclines -4

Chlortetracycline; Doxycycline; Oxytetracycline; Tetracycline

In house Method “VKB-TL-02 Rev.No:01” (Modified from: Journal of Chromatography B 864; 156-160; 2008,

AOAC 997.04 and Journal Pharmaceutical and Biomedical Analysis 64-65; 40-48; 2012

Drinking Water for animals

Analysis of Selected Veterinary Drug Residues-

LC-MS/MS Method

Amphenicols -3

Chloramphenicol; Florfenicol; Thiamphenicol

Anticoccidials -11

Amprolium; Diclazuril; Halofuginone; Lasalocid; Maduramicin; Monensin; Narasin; Nicarbazin; Robenidine; Salinomycin; Toltrazuril.

Diaminopyrimidines -1

Trimethoprim

Quinolones -6

Ciprofloxacin; Danofloxacin; Difloxacin; Enrofloxacin; Flumequin; Sarafloxacin

Lincosamides -1

Lincomycin

Macrolides - 5

Erythromycin; Spiramycin; Tilmicosin; Tylosin; Tylvalosin

Nitrofurans -3

Furaltadone; Furazolidone; Nitrofurantoin

Penicillins -3

Amoxicillin; Dicloxacillin; Penicillin G

Pleuromutilins -1

Tiamulin

Quinoxalines -2

Carbadox; Olaquindox

Streptogramins -1

Virginamycin

Sulfanamides -10

Sulfachloropyridazine; Sulfadiazine; Sulfadimethoxine; Sulfadoxine; Sulfamerazine; Sulfamethazine; Sulfamethoxazole; Sulfapyridine; Sulfaquinoxaline; Sulfathiazole

Tetracyclines -4

Chlortetracycline; Doxycycline; Oxytetracycline; Tetracycline

In House Method “VKB-TL-03 Rev. No:00” (Modified from: Analytica Chimica Acta 700 (2011) 26-33 and AOAC 997.04 modified)

Meat

Analysis of Selected Veterinary Drug Residues-

LC-MS/MS Method

Amphenicols -2

Chloramphenicol; Florfenicol

Anthelmentics -5

Doramectin; Levamisole; Moxidectine; Thiabendazole-5-hydroxy; Thiabendazole

Anticoccidials -6

Lasolacid; Maduramicine; Monensin; Narasin; Nicarbazine; Salinomycin

Quinolones -9

Ciprofloxacin; Danofloxacin; Difloxacin; Enrofloxacin; Flumequine; Marbofloxacin; Nalidixic Acid; Oxolinic Acid; Sarafloxacin

Macrolides -2

Spiramycin; Tilmicosin

Nitroimidazoles -6

Dimetridazole; Ipronidazole-hydroxy; Ipronidazole; Metronidazole; Metronidazole Hydroxy; Ronidazole

NSAIDs -2

Diclofenac; Meloxicam

Penicillins -7

Amoxicillin; Ampicillin; Cephapirin; Dicloxacillin; Penicilline G; Nafcillin, Oxacillin

Sulfanamides -10

Sulfachloropyridazine; Sulfadiazine; Sulfadimethoxine; Sulfadoxine; Sulfamerazine; Sulfamethazine; Sulfamethoxazole; Sulfaquinoxaline; Sulfapyiridine; Sulfathiazole

Tetracyclines -4 Adet

Chlortetracycline; Doxycycline; Oxytetracycline; TetracyclineChlortetracycline; Doxycycline; Oxytetracycline; Tetracycline

In House Method “VKB- TL-04 Rev. No:00”

(Modified from: Multi- residue quantitation of veterinary drugs in animal tissue using optimized solid phase extraction protocol; 8th Workshop on Environmental Applications and Food Safety. Barcelona; Spain; 2-4 July 2012.and Agilent Bond Elut QuEChERS EN Kits by LC/MS/MS; 2012)

Meat

Analysis of Selected Veterinary Drug Residues-

LC-MS/MS Method

A1-Stilbens- 3

Dienestrol; Diethylstilbestrol; Hexestrol

A3-Steroids -3

17-alpha-Methyltestosterone; Melengestrol acetate; Trenbolone

A4-Resorsilicic acid lactones-6

Zearalanone; Zearalenone; Zeranol (Alfa Zearalanol); α-Zearalenol; β-Zearalanol (Taleranol); β-Zearalenol

A5-Betaagonists-4

Cimbuterol; Clenbuterol; Mapenterol; Salbutamol

In House Method “VKB-TL-05 Rev. No:03” (Modified from: Journal of Chromatography B; 2013; 940; 15-23)

Fish

Analysis of Selected Veterinary Drug Residues-

LC-MS/MS Method

A1-Stilbens – 3

Dienestrol; Diethylstilbestrol; Hexestrol

A3-Steroids -3

17-alpha-Methyltestosterone; Melengestrol acetate; Trenbolone

A4-Resorsilicic acid lactones -6

Zearalanone; Zearalenone; Zeranol (Alfa Zearalanol); α-Zearalenol; β-Zearalanol (Taleranol); β-Zearalenol

In House Method “VKB-TL-05 Rev. No:03” (Modified from: Journal of Chromatography B; 2013; 940; 15-23)

Poultry Muscle

Analysis of Selected Veterinary Drug Residues-

LC-MS/MS Method

A1-Stilbens - 3

Dienestrol; Diethylstilbestrol; Hexestrol

A3-Steroids -3

17-alpha-Methyltestosterone; Melengestrol acetate; Trenbolone

A4-Resorsilicic acid lactones -6

Zearalanone; Zearalenone; Zeranol (Alfa Zearalanol); α-Zearalenol; β-Zearalanol (Taleranol); β-Zearalenol

In House Method “VKB-TL-05 Rev. No:03” (Modified from: Journal of Chromatography B; 2013; 940; 15-23)

Poultry Muscle

Analysis of Selected Veterinary Drug Residues-

LC-MS/MS Method

Amphenicols -3

Chloramphenicol; Florfenicol; Thiamfenicol

Anticoccidials- 7

Amprolium; Decoquinate; Diclazuril; Halofuginone; Monensin; Robenidine; Toltrazuril Sulfone

Avermectins-3

Abamectin; Eprinomectin; Ivermectin

Benzimidazoles-11

Albendazole; Albendazole Sulfone; Albendazole Sulfoxide; Albendazole-2-aminosulfone; Cambendazole; Flubendazole; Ketotriclabendazole; Levamisol; Thiabendazole; Thiabendazole-5-Hydroxy; Triclabendazole

Diaminopyrimidines- 1

Trimethoprim

Quinolones - 9

Ciprofloxacin; Danofloxacin; Difloxacin; Enrofloxacin; Flumequine; Marbofloxacin; Nalidixic Acid; Oxolinic Acid; Sarafloxacin

Lincosamides - 1

Lincomycin

Macrolides 6

Erythromycin; Neospiramycin; Spiramycin; Tilmicosin; Tylosin; Tylvalosin

Nitroimidazoles - 4

Ipronidazole Hydroxy; Metronidazole; Metronidazole Hydroxy; Ronidazole

NSAIDs - 5

Carprofen; Diclofenac; Flunixin; Meloxicam; Phenylbutazone

Penicillins - 7 Adet

Cephapirin; Cloxacillin; Dicloxacillin; Nafcillin; Oxacillin; Penicillin G (Benzylpenicillin); Phenoxymethyl Penicillin (Penicillin V)

Quinolones - 1

3-Methylquinoxaline-2-carboxylic acid (MQCA)

Sulfanamides - 10

Sulfachloropyridazine; Sulfadiazine; Sulfadimethoxine; Sulfadoxine; Sulfamerazine; Sulfamethazine; Sulfamethoxazole; Sulfapyridine; Sulfaquinoxaline; Sulfathiazole

Tetracyclines 6

Doxycycline; Epitetracycline; Oxytetracycline; Tetracycline; 4-epi-Chlortetracycline; 4-epi-Oxytetracycline

In House Method “VKB-TL-11 Rev. No:00”

(Modified from: Barnes ve ark. 2008. 8th Workshop on Environmental Applications and Food Safety. 2-4 July 2012. Barcelona, Spain and Zhao ve ark.

Determination of Sulfonamide Antibiotics in Bovine Liver Using Agilent Bond Elut QuEChERS EN Kits by LC/MS/MS, 2012)

Food (Milk Powder, Whey Powder)

Analysis of Selected Veterinary Drug Residues-

LC-MS/MS Method

Macrolides -6

Erythromycin; Spiramycin; Neospiramycin; Tilmicosin; Tylosin; Tylvalosin

Quinolones -9

Ciprofloxacin; Danofloxacin; Difloxacin; Enrofloxacin; Flumequin; Sarafloxacin; Marbofloxacin; Nalidixic Acid; Oxolinic Acid

Lincosamides -1

Lincomycin

Sulfanamides -10

Sulfachloropyridazine; Sulfadiazine; Sulfadimethoxine; Sulfadoxine; Sulfamerazine; Sulfamethazine; Sulfamethoxazole; Sulfapyridine; Sulfaquinoxaline; Sulfathiazole

Diaminopyrimidines-1

Trimethoprim

In House Method “VKB-TL-10 Rev. No 00” (Modified from: Analyitica Chimica Acta. 2015 Jun 23;880:103-21)

Food (Fish)

Analysis of Selected Veterinary Drug Residues- LC-MS/MS Method

Nitroimidazoles-7

Ronidazole; Dimetridazole; Metronidazole; Metronidazole Hydroxy; Ipronidazole; Ipronidazole Hyrodxy; HMMNI (2-Hydroxymethyl-1-methyl-5-nitro-1H- imidazole);

Amfenicols-3

Chloramphenicol; Florfenicol; Thiamfenicol

Tetracyclines-7

Doxycycline; Tetracycline; Epitetracycline; Chlortetracycline; 4-epi-Chlortetracycline; Oxytetracycline; 4-epi-Oxytetracycline

Quinolones-6

Danofloxacin; Difloxacin; Enrofloxacin; Flumequine; Oxolinic Acid; Sarafloxacin

Macrolides-2

Tilmicosin; Tylosin

β-Lactams-5

Oxacillin; Penicilline G (Benzylpenicillin); Ampicillin; Dicloxacillin; Cloxacillin

In House Method “VKB-TL-19 Rev. No 03"

(Modified from: -Multi- residue quantitation of veterinary drugs in animal tissue using optimized solid phase extraction protocol; 8th Workshop on Environmental Applications and Food Safety. Barcelona; 2-4 July 2012 Spain; 2008. -Agilent Bond Elut QuEChERS EN Kits by LC/MS/MS; 2012)

Feed and raw materials of feed

Determination of Crude fibre

AOCS Ba 6a-05

Feed and raw materials of feed

Determination of Crude fat

AOCS Am 5-04

Feed and raw materials of feed

Determination of Total fat

In-house Method –“YMB-TL-33 Rev. No:03”(Modified from: ANKOM Acid Hydrolysis Application Note)

Feed and raw materials of feed

Determination of Total phosphorus

Spectrophotometric method

Regulation on Sampling and Analysis Methods for Official Control of Feeds, Official Gazette No. 29955

Feed and raw materials of feed

Analysis of Water-soluble chlorides (NaCl)

Titrimetric method

Akyıldız, 1968. Feed Science Laboratory Manual, p. 133-134.

Feed and raw materials of feed

Determination of Total sugars

Luff-Schoorl Method

Regulation on Sampling and Analysis Methods for Official Control of Feeds, Official Gazette No. 29955

Feed and Raw Materials of Feed; Feed Additives

Determination of Crude fat

Regulation on Sampling and Analysis Methods for Official Control of Feeds, Official Gazette No. 29955

Feed and Raw Materials of Feed; Feed Additives

Determination of Fibre

AOAC 962.09

Feed and Raw Materials of Feed; Feed Additives

Determination of Crude Ash

TS ISO 5984

Feed and Raw Materials of Feed; Feed Additives

Analysis of Ash Insoluble in HCl

Regulation on Sampling and Analysis Methods for Official Control of Feeds, Official Gazette No. 29955

Feed and Raw Materials of Feed; Feed Additives

Determination of Crude protein

Combustion Method (Dumas Principle)

AOAC 990.03

Feed and Raw Materials of Feed; Feed Additives

Determination of Dry Matter and Moisture

Regulation on Sampling and Analysis Methods for Official Control of Feeds, Official Gazette No. 29955

Feed and Raw Materials of Feed; Feed Additives

Determination of Starch

Polarimetric method

Regulation on Sampling and Analysis Methods for Official Control of Feeds, Official Gazette No. 29955

Feed and Raw Materials of Feed; Feed Additives

Determination of Urea

Spectrophotometric method

TS 10338

Cereal Grains Feed’s Raw Material

Determination of Dry matter and moisture

TS EN ISO 712-1

Food, Environmental Samples Taken from the Food Processing Facility

Aeorobic Colony Count

AOAC 2008.10

bioMérieux TEMPO, AC

Food (Except foods with high enzymatic activity, raw red offal and raw mollusks)

Escherichia coli Count

AOAC 2009.02

bioMérieux TEMPO EC

Food (except fruit purees, cocoa)

Coliform Bacteria Count

AOAC 2008.10

bioMérieux TEMPO TC

Food (excluding fruit purees, cocoa, raw mushrooms, powdered milk, cereals, instant soups, ready-to-use cake mixes)

Coagulase Positive Staphylococcus Count

AOAC 2009 bioMérieux

TEMPO STA

Food (excluding fruit purees, cocoa, raw mushrooms, and beverages)

Enterobactericeae Count

AOAC 2008 bioMérieux

TEMPO; EB

Food (except fruit purees, cocoa, fermented products, and yogurt)

Yeast and Mould Count

AOAC 2010 bioMérieux

TEMPO; YM

Food

Escherichia coli O157 Detection

bioMérieux VIDAS UP O157 ECPT

Food

Listeria monocytogenes Detection

AOAC 2013.11;

bioMérieux VIDAS LMX

Food, Feed

Detection of Salmonella spp.

AOAC 2013.01

bioMérieux VIDAS UP SPT

Food, Feed

Detection of Salmonella spp.

TS EN ISO 6579-1

Food, Feed

Aerobic Colony Count

Pour Plate Technique

ISO 4833-1

Food, Feed

Escherichia coli Count

Colony Count technique

ISO 16649-2

Food, Feed

Coliform Bacteriae Count

Colony Count technique

ISO 4832

Food, Feed

Listeria monocytogenes ((Listeria spp.) detection

ISO 11290-1

Food, Feed

Yeast and mould Count

Colony Count Technique

ISO 21527-1

ISO 21527-2

Food, Feed

Coagulase Positive Staphylococcus Count -(Staphylococcus aureus and other spe)

Colony Count Technique

TS 6582-2 EN ISO 6888-1

TS 6582-2 EN ISO 6888-2

Food, Feed

Clostridium perfringens (Clostridium spp.)

Count Colony Count Technique

TS EN ISO 7937

Food, Feed

Vibrio spp Detection; Vibrio cholera and Vibrio parahaemolyticus Detection

ISO/TS 21872-1

Raw Milks

Somatic Cell Count

TS EN ISO 13366-1

Food, Feed, Environmental Samples taken From Food Plants

Enterobacteriaceae Count

ISO 21528-2

ISO 21528-1

Food

Bacillus cereus Count

Colony Count technique

TS EN ISO 7932

Food

Bacillus cereus Count

AOAC 071401;

bioMérieux TEMPO BC

Water

Colony Count

TS EN ISO 6222

Water

Fecal Enterococcus Count

Most Probable Number Technique

SM 9230 B

Water

Coliform Bacteria Count

Most Probable Number Technique

ISO 9308-2

Water

Escherichia coli (E.coli) Count

Most Probable Number Technique

ISO 9308-2

Water

Enterococcus Fecal Streptecoccus Count

Most Probable Number Technique

TS EN ISO 7899-1

Water

Salmonella Spp. Detection

Membrane Filtration Method

ISO 19250

Food (except milk and dairy product)

B-Glucuronidase Positive E. coli Count

Most Probable Number Technique

ISO/TS 16649-3

Food, Feed and Food Contact Surfaces

Escherichia coli Count

Most Probable Number Technique

ISO 7251

Food, Feed and Environmental Samples Taken from the Food Processing Facility

Enumeration of anaerobic bacteria inducing sulphide

Colony count technique

ISO 15213-1

Food, Feed and Seed

Identification and Quantification Analysis of Soybean Event MON89788

Real Time PCR Metod

Pre-treatment: DNA Extraction

EURL Method (QT-EVE- GM-006), ISO 21570, ISO 24276

Kit Method (Eurofins GENESpin DNA Isolation Kit, Bosphore Plant DNA Extraction Spin Kit) ISO 21571

Food, Feed and Seed

Identification and Quantification Analysis of Cotton Event MON15985

Real Time PCR Metod

Pre-treatment: DNA Extraction

EURL Method (QT-EVE- GH-005), ISO 21570, ISO 24276

Kit Method (Eurofins GENESpin DNA Isolation Kit, Bosphore Plant DNA Extraction Spin Kit) ISO 21571

Food, Feed and Seed

Identification and Quantification Analysis of Cotton Event MON1445

Real Time PCR Metod

Pre-treatment: DNA Extraction

EURL Method (QT-EVE- GH-003), ISO 21570, ISO 24276

Kit Method (Eurofins GENESpin DNA Isolation Kit, Bosphore Plant DNA Extraction Spin Kit) ISO 21571

Food, Feed and Seed

Identification and Quantification Analysis of Cotton Event MON531

Real Time PCR Metod

Pre-treatment: DNA Extraction

EURL Method (QT-EVE- GH-004), ISO 21570, ISO 24276

Kit Method (Eurofins GENESpin DNA Isolation Kit, Bosphore Plant DNA Extraction Spin Kit) ISO 21571

Food, Feed and Seed

Identification and Quantification Analysis of Soybean Event MON-40-3-2

Real Time PCR Metod

Pre-treatment: DNA Extraction

EURL Method (QT-EVE- GM-005), ISO 21570, ISO 24276

Kit Method (Eurofins GENESpin DNA Isolation Kit, Bosphore Plant DNA Extraction Spin Kit) ISO 21571

Food, Feed and Seed

Identification and Quantification Analysis of Oilseed Rape Event RT73

Real Time PCR Metod

Pre-treatment: DNA Extraction

EURL Method (QT-EVE- BN-004), ISO 21570, ISO 24276

Kit Method (Eurofins GENESpin DNA Isolation Kit, Bosphore Plant DNA Extraction Spin Kit) ISO 21571

Food, Feed and Seed

Identification and Quantification Analysis of Sugar Beet Event H7-1

Real Time PCR Metod

Pre-treatment: DNA Extraction

EURL Method (QT-EVE- BV-001), ISO 21570, ISO 24276

Kit Method (Eurofins GENESpin DNA Isolation Kit, Bosphore Plant DNA Extraction Spin Kit) ISO 21571

Food, Feed and Seed

Identification and Quantification Analysis of Soybean Event A2704-12

Real Time PCR Metod

Pre-treatment: DNA Extraction

EURL Method (QT-EVE- GM-004), ISO 21570, ISO 24276

Kit Method (Eurofins GENESpin DNA Isolation Kit, Bosphore Plant DNA Extraction Spin Kit) ISO 21571

Food, Feed and Seed

Identification and Quantification Analysis of Maize Event MIR604

Real Time PCR Metod

Pre-treatment: DNA Extraction

EURL Method (QT-EVE- ZM-013), ISO 21570, ISO 24276

Kit Method (Eurofins GENESpin DNA Isolation Kit, Bosphore Plant DNA Extraction Spin Kit) ISO 21571

Food, Feed and Seed

Identification and Quantification Analysis of Maize Event Bt11

Real Time PCR Metod

Pre-treatment: DNA Extraction

EURL Method (QT-EVE- ZM-015), ISO 21570, ISO 24276

Kit Method (Eurofins GENESpin DNA Isolation Kit, Bosphore Plant DNA Extraction Spin Kit) ISO 21571

Food, Feed and Seed

Identification and Quantification Analysis of Oilseed Rape Event T45

Real Time PCR Metod

Pre-treatment: DNA Extraction

EURL Method (QT-EVE- BN-001), ISO 21570, ISO 24276

Kit Method (Eurofins GENESpin DNA Isolation Kit, Bosphore Plant DNA Extraction Spin Kit) ISO 21571

Food, Feed and Seed

Identification and Quantification Analysis of Oilseed Rape Event RF3

Real Time PCR Metod

Pre-treatment: DNA Extraction

EURL Method (QT-EVE- BN-003), ISO 21570, ISO 24276

Kit Method (Eurofins GENESpin DNA Isolation Kit, Bosphore Plant DNA Extraction Spin Kit) ISO 21571

Food, Feed and Seed

Identification and Quantification Analysis of Oilseed Rape Event MS8

Real Time PCR Metod

Pre-treatment: DNA Extraction

EURL Method (QT-EVE- BN-002), ISO 21570, ISO 24276

Kit Method (Eurofins GENESpin DNA Isolation Kit, Bosphore Plant DNA Extraction Spin Kit) ISO 21571

Food, Feed and Seed

Identification and Quantification Analysis of Soybean Event MON87701

Real Time PCR Metod

Pre-treatment: DNA Extraction

EURL Method (QT-EVE- GM-010), ISO 21570, ISO 24276

Kit Method (Eurofins GENESpin DNA Isolation Kit, Bosphore Plant DNA Extraction Spin Kit) ISO 21571

Food, Feed and Seed

Identification and Quantification Analysis of Soybean Event A5547-127

Real Time PCR Metod

Pre-treatment: DNA Extraction

EURL Method (QT-EVE- GM-007), ISO 21570, ISO 24276

Kit Method (Eurofins GENESpin DNA Isolation Kit, Bosphore Plant DNA Extraction Spin Kit) ISO 21571

Food, Feed and Seed

Identification and Quantification Analysis of Soybean Event DP-356043-5

Real Time PCR Metod

Pre-treatment: DNA Extraction

EURL Method (QT-EVE- GM-009), ISO 21570, ISO 24276

Kit Method (Eurofins GENESpin DNA Isolation Kit, Bosphore Plant DNA Extraction Spin Kit) ISO 21571

Food, Feed and Seed

Identification and Quantification Analysis of Maize Event 3272

Real Time PCR Metod

Pre-treatment: DNA Extraction

EURL Method (QT-EVE- ZM-019), ISO 21570, ISO 24276

Kit Method (Eurofins GENESpin DNA Isolation Kit, Bosphore Plant DNA Extraction Spin Kit) ISO 21571

Food, Feed and Seed

Identification and Quantification Analysis of Cotton Event 281-24-236

Real Time PCR Metod

Pre-treatment: DNA Extraction

EURL Method (QT-EVE- GH-001A), ISO 21570,

ISO 24276

Kit Method (Eurofins GENESpin DNA Isolation Kit, Bosphore Plant DNA Extraction Spin Kit) ISO 21571

Food, Feed and Seed

Identification and Quantification Analysis of Cotton Event 3006-210-23

Real Time PCR Metod

Pre-treatment: DNA Extraction

EURL Method (QT-EVE- GH-001B), ISO 21570,

ISO 24276

Kit Method (Eurofins GENESpin DNA Isolation Kit, Bosphore Plant DNA Extraction Spin Kit) ISO 21571

Food, Feed and Seed

Identification and Quantification Analysis of Cotton Event LLCOTTON25

Real Time PCR Metod

Pre-treatment: DNA Extraction

EURL Method (QT-EVE- GH-002), ISO 21570, ISO 24276

Kit Method (Eurofins GENESpin DNA Isolation Kit, Bosphore Plant DNA Extraction Spin Kit) ISO 21571